A Review of the Most Important Methods for Severe Plastic Deformation of Titanium

Subject Areas : journal of New Materials

Sayyed Mohammadreza Sedehi ¹ (School of Mechanical Engineering, College of Engineering, University of Tehran, Tehran, Iran)
Mohammadreza Maraki ² (Department of Materials Engineering, Birjand University of Technology, Birjand, Iran)
Ali Jalali ³ (Department of Mechanical Engineering, Birjand University of Technology, Birjand, Iran)
Hadi Ezadi ⁴ (Department of Mechanical Engineering, Birjand University of Technology, Birjand, Iran)

Received: 2023-12-23 Accepted : 2024-02-07 Published : 2023-07-23

Keywords: accumulative roll bonding, Severe plastic deformation, Simple shear extrusion, equal channel angular pressing, Titanium,

Abstract :

Abstract In recent years, extensive studies have been conducted on severe plastic deformation based on suitable processes for sheets and solid materials. Considering the limitations in some properties and crucial applications of titanium metal, these methods are considered intriguing avenues for enhancing the efficiency of this practical metal. Therefore, efforts have been made to investigate and develop effective severe plastic deformation processes for producing titanium samples. Severe plastic deformation is widely recognized as the primary method for producing ultrafine and nanostructured materials with high strength and hardness. This study focuses on exploring the most recent methods in this family suitable for producing nanostructured titanium samples with ultrafine grains. Furthermore, the study assesses the impact of several key severe plastic deformation methods on titanium properties, comparing them based on the advantages and disadvantages of these methods from both processing and property perspectives. Findings: In this regard, in recent years, severe plastic deformation methods have been introduced and extensively studied. In this research, by examining and reviewing the latest studies related to the advantages and disadvantages of three methods: simple shear extrusion, accumulative roll bonding, and equal channel angular pressing, the following results have been obtained : All past research indicates that these three methods have a significant and positive impact on the mechanical properties of titanium metal. These positive effects show an increasing acceleration up to a certain number of passes and then reach a saturation point. Temperature, speed, and appropriate processing are three fundamental and important factors concerning severe plastic deformation of titanium metal. Some studies suggest that pure titanium metal can also be processed at room temperature using methods of severe plastic deformation. The frequency of using these methods in relation to titanium metal and its alloys includes methods such as ECAP, accumulative roll bonding, and simple shear extrusion, respectively. A noticeable weakness in most studies conducted on processed titanium using severe plastic deformation methods is the lack of investigation into the biocompatibility properties of titanium concurrently with its mechanical properties after the process. 6. It can be almost stated that in none of the studies conducted on severe plastic deformation methods, a specific industrial output has been introduced, and it remains at the level of research work.

References:

1. Maghsoudloo, H., Gerdooei, M., & Ghaderi, S. H. (2019). Improving Mechanical Properties of Ultrafine-Grained Titanium Produced through Warm ECAP Using a Novel Lubrication System. Amirkabir Journal of Mechanical Engineering, 51(5), 1047-1056.

2. Eftekhari M, Faraji G, Shapoorgan O, Baniassadi M. Experimental investigation of the effect of temperature in extrusion process of ECAPed nanostructured Titanium. Modares Mechanical Engineering. 2017 Jun 10;17(4):52-60.

3.  R.Z. Valiev, I.P. Semenova, V.V. Latysh, H. Rack, T.C. Lowe, J. Petruzelka, L. Dluhos, D. Hrusak, J. Sochová, Nanostructured titanium for biomedical applications, Advanced engineering materials, 10(8) (2008).

4. Y. Okazaki, E. Gotoh, Comparison of metal release from various metallic biomaterials in vitro, Biomaterials, 26(1) (2005) 11-21.

5. Y. Li, C. Wong, J. Xiong, P. Hodgson, C. Wen, Cytotoxicity of titanium and titanium alloying elements, Journal of dental research, 89(5) (2010) 493-497.

6. Balasubramanian, R., Nagumothu, R., Parfenov, E., Valiev, R., 2021. Development of nanostructured titanium implants for biomedical implants – a short review. Mater. Today Proc. https://doi.org/10.1016/j.matpr.2021.02.064.

7. Polyakov, A.V., Dluhoˇ s, L., Dyakonov, G.S., Raab, G.I., Valiev, R.Z., 2015. Recent advances in processing and application of nanostructured titanium for dental implants. Adv. Eng. Mater. 17, 1869–1875. https://doi.org/10.1002/ adem.201500212.

8. Aktas, S., Kisioglu, Y., 2022. Improving the fatigue life of produced dental implants by the thread-rolling process. Mater. Test. 64, 1012–1025. https://doi.org/10.1515/mt- 2021-2159.

9. Sedehi SM, Khosravi M, Yaghoubinezhad Y. Mechanical properties and microstructures of reduced graphene oxide reinforced titanium matrix composites produced by spark plasma sintering and simple shear extrusion. Ceramics International. 2021 Dec 1;47(23):33180-90.

10. Ansarian, I., Shaeri, M.H., Ebrahimi, M., Min´ arik, P., Bartha, K., 2019. Microstructure evolution and mechanical behaviour of severely deformed pure titanium through multi directional forging. J. Alloys Compd. 776, 83–95. https://doi.org/10.1016/j. jallcom.2018.10.196.

11. Attarilar, S., Djavanroodi, F., Irfan, O.M., Al-Mufadi, F.A., Ebrahimi, M., Wang, Q.D., 2020. Strain uniformity footprint on mechanical performance and erosion-corrosion behavior of equal channel angular pressed pure titanium. Results Phys. 17, 103141 https://doi.org/10.1016/j.rinp.2020.103141.

12. Nosrati, Hasan Ghaforian, Mahdi Gerdooei, Khalil Khalili, and Majid Mohammadi. "Usability of the ECAP-Conform process for the production of dental implants material." Journal of the Mechanical Behavior of Biomedical Materials 147 (2023): 106124.

13. Bodkhe M, Sharma S, Mourad AH, babu Sharma P. A review on SPD processes used to produce ultrafine-grained and multilayer nanostructured tubes. Materials Today: Proceedings. 2021 Jan 1;46:8602-8.

14. Valder J, Rijesh M, Surendranathan AO. Forming of tubular commercial purity aluminum by ECAP. Materials and Manufacturing Processes. 2012 Sep 1;27(9):986-9.

15. M.I. Babaghayou, A.-H.-I. Mourad, A. Ochoa, Freddys Beltrán, and Nizamudeen Cherupurakal. ‘‘Study on the thermal stability of stabilized and unstabilized low-density polyethylene films.”, Polym. Bull. (2020) 1–17.

16. Pardis N, Ebrahimi R. Deformation behavior in Simple Shear Extrusion (SSE) as a new severe plastic deformation technique. Materials Science and Engineering: A. 2009 Dec 15;527(1-2):355-60.

17. Pardis N, Ebrahimi R. Deformation behavior in Simple Shear Extrusion (SSE) as a new severe plastic deformation technique. Materials Science and Engineering: A. 2009 Dec 15;527(1-2):355-60.

18. Sheikh H, Ebrahimi R, Bagherpour E. Crystal plasticity finite element modeling of crystallographic textures in simple shear extrusion (SSE) process. Materials & Design. 2016 Nov 5;109:289-99.

19. Bagherpour E, Qods F, Ebrahimi R, Miyamoto H. Microstructure evolution of pure copper during a single pass of simple shear extrusion (SSE): role of shear reversal. Materials Science and Engineering: A. 2016 Jun 1;666:324-38.

20. Sedehi, S. M. R., Khosravi, M., Yaghoubinezhad, Y., “Experimental investigation of mechanical properties, corrosion and biocompatibility of Ti/RGO composite made by the combined method of spark plasma sintering and simple shear extrusion,” In Persian, Journal of Science and Technology of Composites, Vol. 9, No. 1, pp. 1921-1926, 2022. https://doi.org/10.22068/JSTC.2022.559027.797

21. Semenova IP, Polyakova VV, Dyakonov GS, Polyakov AV. Ultrafine‐Grained Titanium‐Based Alloys: Structure and Service Properties for Engineering Applications. Advanced Engineering Materials. 2020 Jan;22(1):1900651.

22. Jäger A, Gärtnerova V, Tesař K. Microstructure and anisotropy of the mechanical properties in commercially pure titanium after equal channel angular pressing with back pressure at room temperature. Materials Science and Engineering: A. 2015 Sep 17;644:114-20.

23. Wu Y, Feng F, Xin H, Li K, Tang Z, Guo Y, Qin D, An B, Diao X, Dou C. Fracture strength and osseointegration of an ultrafine-grained titanium mini dental implant after macromorphology optimization. ACS Biomaterials Science & Engineering. 2019 Jun 20;5(8):4122-30.

24. Shaat M. Effects of processing conditions on microstructure and mechanical properties of equal-channel-angular-pressed titanium. Materials Science and Technology. 2018 Jul 3;34(10):1149-67.

25. Gu Y, Ma A, Jiang J, Yuan Y, Wu H. Microstructure and tensile anisotropy of pure Ti processed by up-scaled RD-ECAP. Materials Characterization. 2020 Oct 1;168:110513.

26. Németh G, Horváth K, Hervoches C, Cejpek P, Palán J, Duchek M, Máthis K. Characterization of the Microstructure, Local Macro-Texture and Residual Stress Field of Commercially Pure Titanium Grade 2 Prepared by CONFORM ECAP. Metals. 2018 Nov 29;8(12):1000.

[27] Hoseini M, Pourian MH, Bridier F, Vali H, Szpunar JA, Bocher P. Thermal stability and annealing behaviour of ultrafine grained commercially pure titanium. Materials Science and Engineering: A. 2012 Jan 15;532:58-63.

28. Hajizadeh K, Alamdari SG, Eghbali B. Stored energy and recrystallization kinetics of ultrafine grained titanium processed by severe plastic deformation. Physica B: Condensed Matter. 2013 May 15;417:33-8.

29. Tesař K, Koller M, Vokoun D, Tyc O, Čech J, Sedlák P. Texture, elastic anisotropy and thermal stability of commercially pure titanium prepared by room temperature ECAP. Materials & Design. 2023 Feb 1;226:111678.

30. Gu Y, Ma A, Jiang J, Li H, Song D, Wu H, Yuan Y. Simultaneously improving mechanical properties and corrosion resistance of pure Ti by continuous ECAP plus short-duration annealing. Materials Characterization. 2018 Apr 1;138:38-47.

31. State Key Laboratory of Metal Matrix Composites, Shanghai Jiao Tong University, Shanghai 200240, PR China (W. Lu).

32. Qarni MJ, Rosochowski A, Boczkal S. Influence of incremental ECAP on the microstructure and tensile behaviour of commercial purity titanium. Procedia engineering. 2017 Jan 1;207:1481-6.

33. Jafarian HR, Mahdavian MM, Shams SA, Eivani AR. Microstructure analysis and observation of peculiar mechanical properties of Al/Cu/Zn/Ni multi-layered composite produced by Accumulative-Roll-Bonding (ARB). Materials Science and Engineering: A. 2021 Feb 23;805:140556.

34. Wei Z, Zheng H, Wu R, Zhang J, Wu H, Jin S, Jiao Y, Hou L. Interface behavior and tensile properties of Mg-14Li-3Al-2Gd sheets prepared by four-layer accumulative roll bonding. Journal of Manufacturing Processes. 2021 Jan 1;61:254-60.

35. Ye N, Ren X, Liang J. Microstructure and mechanical properties of Ni/Ti/Al/Cu composite produced by accumulative roll bonding (ARB) at room temperature. Journal of Materials Research and Technology. 2020 May 1;9(3):5524-32.

36. Gholami MD, Salamat M, Hashemi R. Study of mechanical properties and wear resistance of Al 1050/Brass (70/30)/Al 1050 composite sheets fabricated by the accumulative roll bonding process. Journal of Manufacturing Processes. 2021 Nov 1;71:407-16.

37. Roghani H, Borhani E, Jafarian HR. Effect of a trace amount addition of CuO on aluminum sheet processed by accumulative roll bonding with the common roots and rapid annealing. Journal of Materials Research and Technology. 2021 Nov 1;15:4257-71.

38.  Roghani H, Borhani E, Shams SA, Lee CS, Jafarian HR. Effect of concurrent accumulative roll bonding (ARB) process and various heat treatment on the microstructure, texture and mechanical properties of AA1050 sheets. Journal of Materials Research and Technology. 2022 May 1;18:1295-306.

39. Ghafari-Gousheh S, Nedjad SH, Khalil-Allafi J. Tensile properties and interfacial bonding of multi-layered, high-purity titanium strips fabricated by ARB process. Journal of the Mechanical Behavior of Biomedical Materials. 2015 Nov 1;51:147-53.

40.  Kitahara H, Matsushita S, Tsushida M, Ando S, Tsuji N. Fatigue properties of ARB-processed Ti sheets with crystallographic texture. International Journal of Fatigue. 2016 Nov 1;92:18-24.

41. فلاحتی عقدا, صفا, and حاجی صفری. "بررسی فرآیند PEO بر رفتار خستگی آلیاژ تیتانیوم Ti-6Al-4V." فصلنامه علمی-پژوهشی مواد نوین 8, no. 31 (2018): 141-152.‎

42.  Milner JL, Abu-Farha F, Bunget C, Kurfess T, Hammond VH. Grain refinement and mechanical properties of CP-Ti processed by warm accumulative roll bonding. Materials Science and Engineering: A. 2013 Jan 20;561:109-17

43.  Maghsoudloo, H., Gerdooei, M., Ghaderi, S.H., 2017. Investigation of Mechanical Properties of a Titanium Implant Processed by Equal Channel Angular Pressing. Shahrood University of Technology.

44. Lin, H.K.; Li, G.Y.; Mortier, S.; Bazarnik, P.; Huang, Y.; Lewandowska, M.; Langdon, T.G. Processing of CP-Ti by high-pressure torsion and the effect of surface modification using a post-HPT laser treatment. J. Alloys Compd. 2019, 784, 653–659. [CrossRef]

45. Edalati, K.; Horita, Z. A review on high-pressure torsion (HPT) from 1935 to 1988. Mater. Sci. Eng. A 2016, 652, 325–352. [CrossRef]

46. Bagherpour, E.; Pardis, N.; Reihanian, M.; Ebrahimi, R. An overview on severe plastic deformation: Research status, techniques classification, microstructure evolution, and applications. Int. J. Adv. Manuf. Technol. 2019, 100, 1647–1694. [CrossRef]

47. Gurau, G.; Bujoreanu, L.; Potecasu, O.; Cananau, N.; Alexandru, P.; Gurau, C.; Tanase, D. Process and Machine for Deforming Taper-Shaped Active Elements Made of Shape-Memory Materials by Twisting upon High. Pressure. Patent RO129900, 30 December 2016.